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Sol-Gel Synthesis of Nanomaterials and their applications explains various aspects of nanomaterials along with its sol-gel synthesis. The processing of sol-gel synthesis has been provided in detail which also includes, synthesis and characterization of Perovskite-Type and sol-gel-derived glass-ceramic photorefractive films for photonic structures. Provide the reader with the insights into the development of various applications used for synthesizing nanomaterials, so as to understand the effect of Cerium Ions on the Structure, Porosity and Electrochemical Properties of Si/Zr-Based Hybrid Sol-Gel Coatings Deposited on Aluminum.